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Proceedings Paper

Ablation properties of inorganic filler modified benzoxazine composite coating irradiated by high-intensity continuous laser
Author(s): Feng Xu; Zhuang Ma; Hezhang Li; Lihong Gao; Fuchi Wang
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Paper Abstract

Benzoxazine resin with good heat resistance, low combustion heat release and high char yield is a promising thermosetting resin. Meanwhile, research shows that the inorganic filler can effectively improve the thermodynamic property of the resin. It makes that the inorganic filler modified benzoxazine may have a potential application in laser ablation. The benzoxazine coating with and without inorganic filler ammonium polyphosphate, melamine and pentaerythritol (P-BOZ and BOZ) were prepared by brush and thermal curing method. The ablation properties of these coatings irradiated by high-intensity laser were investigated. The scanning electron microscope, Raman spectroscopy and thermal gravimetric analysis were used to characterize the micrographs, carbon layer structure and thermodynamic property of the sample. Results show that the composite coating has excellent thermal protective properties. The back temperature of 20 wt% P-BOZ coating under different parameter laser power (1000W/cm2, 5s; 1000W/cm2, 10s) are 40% lower than these of the BOZ coating and the 20 wt% P-BOZ has higher mass ablation rate. In the surface layer of the irradiated area, dense carbon layer is produced which reduces the absorb of the laser energy of the interior. In the interior of the sample, a large number of closed bell shaped holes are generated which are beneficial to obstruct the heat conduction.

Paper Details

Date Published: 12 May 2017
PDF: 7 pages
Proc. SPIE 10173, Fourth International Symposium on Laser Interaction with Matter, 1017302 (12 May 2017); doi: 10.1117/12.2268248
Show Author Affiliations
Feng Xu, Beijing Institute of Technology (China)
Zhuang Ma, Beijing Institute of Technology (China)
Hezhang Li, Beijing Institute of Technology (China)
Lihong Gao, Beijing Institute of Technology (China)
Fuchi Wang, Beijing Institute of Technology (China)

Published in SPIE Proceedings Vol. 10173:
Fourth International Symposium on Laser Interaction with Matter
Yongkun Ding; Guobin Feng; Dieter H. H. Hoffmann; Jianlin Cao; Yongfeng Lu, Editor(s)

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