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Proceedings Paper

Preparation of low-density porous silica thin films by ambient pressure drying
Author(s): Lanfang Yao; Jun Shen; Guangming Wu; Xingyuan Ni; Jue Wang; Bin Zhou
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Paper Abstract

Low-density silica thin films having densities ρ of 0.574-0.957(g/cm3 )and refractive indices n of 1.12-1.20 and porosities ∏ of 61%-77% as well as dielectric constants k of 1.92-2.54 were prepared by a two-step sol-gel process at ambient pressure, with a simple dip-coating procedure, which take the wet gel through solvent exchange and reaction with trimethylchlorosilane(TMCS) without any supercritical drying. The process was optimized by varying the dilution, aging, organic substitution, organic modification, heat treatment and dip-coating conditions. Ellipsometer was used to determine refractive index and thickness of films. Atomic force microscopy (AFM) used to observe the microstructure and surface of thin films. Infrared spectroscopy and anti-reflectance measurement was carried out too. Abrasion-resistant properties were tested by the methods suggested by Floch .

Paper Details

Date Published: 8 December 2004
PDF: 4 pages
Proc. SPIE 5774, Fifth International Conference on Thin Film Physics and Applications, (8 December 2004); doi: 10.1117/12.607296
Show Author Affiliations
Lanfang Yao, Tongji Univ. (China)
Univ. of Shanghai for Science and Technology (China)
Jun Shen, Tongji Univ. (China)
Guangming Wu, Tongji Univ. (China)
Xingyuan Ni, Tongji Univ. (China)
Jue Wang, Tongji Univ. (China)
Bin Zhou, Tongji Univ. (China)

Published in SPIE Proceedings Vol. 5774:
Fifth International Conference on Thin Film Physics and Applications
Junhao Chu; Zongsheng Lai; Lianwei Wang; Shaohui Xu, Editor(s)

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