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Proceedings Paper

Reversed phase HPLC-FTIR by on-line extraction and solvent elimination
Author(s): G. W. Somsen; Cees Gooijer; Udo A. T. Brinkman; Nel H. Velthorst; T. Visser
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Paper Abstract

A reversed phase LC-FTIR interface is described using on-line extraction of the aqueous effluent with a volatile organic solvent in conjunction with a solvent eliminating spray-jet device. Results are shown of the analysis of a 2. 10-4 M solution of acenaphthenequinone, phenanthrenequinone and two polar pesticides linuron and diuron. The mixture was separated with a mobile phase of acetonitrile-phosphate buffer and post-column extracted with dichloro-methane. Detection was carried out by FTIR transmission microscopy. The characteristics of the on-line extraction system are discussed in relation to results obtained from a direct deposition method.

Paper Details

Date Published: 31 January 1994
PDF: 2 pages
Proc. SPIE 2089, 9th International Conference on Fourier Transform Spectroscopy, (31 January 1994);
Show Author Affiliations
G. W. Somsen, Free Univ. (Netherlands)
Cees Gooijer, Free Univ. (Netherlands)
Udo A. T. Brinkman, Free Univ. (Netherlands)
Nel H. Velthorst, Free Univ. (Netherlands)
T. Visser, National Institute of Public Health and Environmental Protection (Netherlands)

Published in SPIE Proceedings Vol. 2089:
9th International Conference on Fourier Transform Spectroscopy
John E. Bertie; Hal Wieser, Editor(s)

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