Proceedings Volume 4430

ROMOPTO 2000: Sixth Conference on Optics

cover
Proceedings Volume 4430

ROMOPTO 2000: Sixth Conference on Optics

View the digital version of this volume at SPIE Digital Libarary.

Volume Details

Date Published: 29 June 2001
Contents: 7 Sessions, 121 Papers, 0 Presentations
Conference: ROMOPTO 2000: Sixth Conference on Optics 2000
Volume Number: 4430

Table of Contents

icon_mobile_dropdown

Table of Contents

All links to SPIE Proceedings will open in the SPIE Digital Library. external link icon
View Session icon_mobile_dropdown
  • Laser and Radiation Sources
  • Lasers in Material Sciences
  • Nonlinear, Quantum and Information Optics
  • Biophotonics
  • Optoelectronics
  • Optical Sensors and Metrology
  • Optical Components
Laser and Radiation Sources
icon_mobile_dropdown
Epilogue: a background document about optics for "Physics 2000"
This document was written by the International Commission for Optics, ICO (IUPAP Affiliated Commission AC1) at the invitation of the IUPAP and the International Commission on Physics Education (IUPAP/C14). It explains the major advances in Optics in the last part of this century and makes predictions about how Optics may be expected to develop, and what it might achieve in the next 10-20 years.
Efficient x-ray pulse generation from femtosecond-laser-produced plasma and its application to time-resolved spectroscopy
Hidetoshi Nakano, Tadashi Nishikawa, Naoshi Uesugi
High-density plasmas created near a solid surface by a femtosecond laser pulse emit ultrashort x-ray pulses that are synchronized to the laser pulse. The spectral and temporal properties of x-rays emitted from a femtosecond laser-produced on metal surface are shown. The minimum pulse duration was less than 3 ps. More than a 30-fold enhancement of soft x-ray emission was achieved by fabricating an array of nanoholes on an alumina surface. Utilizing a 10-ps soft x-ray pulse, we demonstrated time-resolved soft x-ray absorption measurement of optically excited silicon near its LII,III edge. We found that a laser pulse irradiation caused a more than 10% increase in soft x-ray absorption near the edge, which recovered within 20 ps.
Frequency stabilization of DBR diode laser against Cs absorption lines at 852 nm using the modulation transfer method
Fabrizio Bertinetto, Paolo Cordiale, Gianluca Galzerano, et al.
Preliminary results on absolute frequency stabilization of Distributed Bragg Reflector (DBR) diode-lasers with emission wavelength at 852 nm will be reported. Saturated absorption D2 lines of cesium atom have been adopted as a frequency reference and the nonlinear spectroscopy method of Modulation Transfer has been used to lock the laser frequency against the resonance. From the preliminary results on the beat signal between two independent laser systems a relative frequency stability of 10-11 has been reached at an integration time of 0.1 s. The analysis on the obtained signal to noise ratio shows a frequency noise floor in the order of approximately 10-12 which should be achieved in an integration time of 1 s.
Lasing without population inversion: efficient frequency up-conversion by incoherent pumping fields
F. F. Popescu
In this paper we have studied the possibility to reach an efficient frequency up-conversion by using two incoherent pumping fields. At the same time, the noise of the generated field is not high, because the generation does not depend on the frequency overlapping, or the phase mismatching of the three involved fields. In this case the system acts as a laser without population inversion. Another advantage of this up-conversion mechanism is the generation of coherent radiation by using incoherent pumping fields. Consequently, the proposed up-conversion mechanism is not limited in frequency by the available coherent radiation for pumping fields. Higher frequency coherent radiation than that obtained up to now could be generated.
Microchip high-power radially pumped composite Yb:YAG laser
Nicolaie A. Pavel, Jiro Saikawa, Sunao Kurimura, et al.
A novel design for a quasi-three level, microchip high-power laser is proposed. The design uses a Yb:YAG core surrounded by an undoped YAG region of slab shape that could be pumped from one or from both slab sides. Theoretical descriptions of the pumping optimization, pump-beam distribution, and output-to-input power characteristics are presented. The simulations show that from a composite Yb:YAG chip, which consists of a Yb:YAG core of 2.0-mm diameter and 13.0-at.% Yb concentration surrounded by an undoped YAG slab of 5.0-mm width and 0.8-mm thickness, a TEM00 output beam of 100 W continuous-wave power could be obtained. The expected optical-to-optical efficiency is 39%.
Wakefield by a short laser pulse
J. Vanchinkhuu, Sinan Bilikmen
The equation describing the plasma response to the acting laser pulse is derived by using the Hamilton-Jacobi equation for the case vg approximately equals vph approximately equals w <EQ c. The equation is solved numerically for one-dimensional Gaussian pulse and analytically for a square-shaped laser pulse. It is shown that the amplitude and the wavelength of the wake wave depend strongly on the amplitude and the length of the laser pulse.
Intrinsic oscillation threshold of 3-um erbium lasers
Serban Georgescu, Claudiu Hapenciuc, Cristian Florea
Mathematical modeling is used to estimate the contribution of the intrinsic oscillation threshold (absence of any lsses) to the threshold of 3-micrometers erbium lasers. For the Er:YAG laser, a strong concentration dependence of this contribution is found.
Nd:YAG laser continuous wave-pumped Q-switched by hybrid passive-active methods
Traian Dascalu, Constanta Dascalu, Nicolaie A. Pavel
The output characteristics of a continuous-wave flash lamp pumped Nd:YAG laser, passively Q-switched by Cr4+:YAG are reported. In order to control the small-signal transmission of the passive Q-switch, a new method, which made use of a miniature laser placed out of the resonator, is described theoretically and proved experimentally. Further, the combination of a Cr4+:YAG passive Q-switch and an acoustooptic Q- switch that work together in a Nd:YAG CW pumped laser was investigated. With a two-rod resonator and a Cr4+:YAG crystal as saturable absorber, an average laser output power over 180W was reached. The pulse-to-pulse stability was 1%. Folded resonator was used in order to obtain intracavity second harmonic generation in active and passive Q-switch mode.
Spectroscopy and energy transfer characteristics of Nd3+ in CNGG
The garnets with disordered structure such as calcium niobium gallium garnet (CNGG) doped with Nd3+ are interesting materials for diode pumping. Spectroscopic investigations on Nd3+:CNGG have revealed a multisite structure and this is reflected in laser emission characteristics. The purpose of this paper is to present several new spectral aspects, a modeling for the main nonequivalent centers, energy transfer characteristics and an attempt to connect the laser characteristics to centers structure. Samples were grown by Czochralski method with Nd3+ from 0.1 to 5 at.% and the high resolution spectral and decay measurements were performed at 10 K. Similar considerations were made in the case of Nd3+ doped in calcium lithium niobium gallium garnet (CLNGG).
Radiation damping in dielectronic recombination of CIV
V. Stancalie, P. G. Burke, V. M. Burke
Radiation damping effect in dielectronic recombination (DR) of CIV is analysed by applying the ab initio, fully nonperturbative R-matrix Floquet theory and its extension to laser induced degenerate states phenomenon. The autoionizing and excited Rydberg states of the complex ion, which are resonantly coupled by the radiation field, are characterized in a Floquet approach by complex quasienergies. By varying the laser intensity and frequency, with overlapping resonances, the interference terms in the expression for dielectronic recombination probability are directly obtained from the calculation.
New model concering the hollow cathode electric discharge (HCED) as a spectral source in mixed noble gases and metal vapors
Iancu Iova, M. Bazavan, Costel Biloiu, et al.
This work concerns with the excitation and ionization processes in the cathode region of the hollow cathode abnormal glow discharge, like in a genetically abnormal glow discharge in mixture of noble gases and metal vapors. The proposed model takes into account the ionic and atomic population of metal vapors, the metastables population of predominant buffer gas and of the ion population of the gas mixture, while the other models, reported in the literature don't take into account the last two populations. This model is qualitatively experimentally attested.
Effect of cooperative atomic interactions on the linewidth of a single-mode laser
M. Mardale, Mariana Craiu, Paul E. Sterian
As the laser linewidth arises under the influence of spontaneous emission, it is of considerable interest to find effects that decrease it. In this paper it is considered the effect of cooperative atomic interactions on the linewidth of a single-mode laser. It can be shown by suitably generalizing the Scully-Lamb theory that the cooperative effects tend to decrease the natural linewidth of the laser at high intensities. Considering the interaction of two-two- level atoms with a single-mode quantized field and the effect of cooperative atomic interactions it was obtained an expression for the natural linewidth of the system. Based on the theoretical models we obtain the numerical results for the laser linewidth as a function of the cooperation parameter. We then present a set of graphs by suitably plotting these data and we discuss the results.
Effects of up-conversion energy transfer on the decay shapes of the 4F3/2 level of Nd3+ in YAG at high-pump intensities
Voicu Lupei, B. Diaconescu, Aurelia Lupei
Experimental data presents a pump intensity dependence of the 4F3/2Nd3+ level emission in various hosts; these effects were assigned to the up-conversion processes. A new formalism that takes into account both up- and down-conversion processes and the statistical distribution of acceptors around donor in the case of direct processes is presented. This involves a time dependent of transfer function and two interaction types: dipolar and superexchange. The profile of excitation beam is considered in order to compare theoretical calculations with experimental data. Calculations concerning quantum efficiency as a function on the ratio between up- and down- conversion rates are presented.
Inhomogeneous broadening by point defects of RE3+ optical lines in YAG
L. Rogobete, Aurelia Lupei, Voicu Lupei, et al.
Most of the RE3+ optical lines in YAG, at low temperature and concentrations, present two interesting features: a multisite structure and Lorenz lineshape of the inhomogeneous broadened lines. The satellite structure of RE3+ ions optical spectra in high temperature YAG present a group of P satellite lines of almost equal intensity that was assigned to nonstoichiometric occupation of Al3+ octahedral sites (a) by Y3+. Up to now, no reliable explanation of the anisotropic effects of Y3+(a) on RE3+ spectra was given. In this paper an attempt is made to explain the multisite structure and lineshapes in terms of the strain field (induced by point defects) theory. The model is illustrated for the absorption line 4I15/2 implies 4S3/2 of Er3+ (1.at.%) doped in YAG.
Transient processes in laser-solid interaction characterized by the induced thermoelectronic current variation
Florenta Costache, O. Toma, Horatiu Totia
Based on the signals produced by the induced thermo- electronic current variation, a study regarding the transient processes in laser-solid interaction was developed. Experiments were performed with a Nd:YAG laser, 100 ns pulses duration, by laser beam focusing onto wolfram samples placed into a vacuum chamber. The amplitude and the temporal variation of resulted signals can conclude about the magnitude order of the temperature decay time due to laser-solid interaction. Therefore, the output signal profile analysis gives information about the time evolution of the transient thermal processes determined by the laser radiation absorption.
Laser mode competition and stability analysis in intensity-time plane
Alina Gearba, Gabriela Cone
It is numerically analyzed the mode competition in a laser with three modes that are oscillating over their threshold, solving the coupled mode equations and following the semiclassical formalism of Lamb. The analysis is started from the stability conditions in different situations of coupling between modes: the weak coupling approximation, the single-mode and two-mode operating and the strong coupling approximation. We plot the trajectories for the coupled oscillators versus time. In our work we assumed homogeneous broadening of the gain medium. This implies that the results apply to a solid-state or a dye laser. For a gas laser, we have to include Doppler broadening and the analysis in this case will be more complicated. The conclusions are that the dynamics of the system can become multistabile and/or unstabile and highly sensitive to the initial conditions and the coupling matrix.
Reciprocity theorem for smith-purcell configurations
Florea Scarlat, M. Facina
The reciprocity theorem is referred to the equivalence of the obtained relations for the Smith-Purcell radiation, in both cases when the electron beam is propagating forward and backward with respect to the metal grating, respectively. The results of the radiation factor for the Smith-Purcell radiation in the ((theta) , (phi) ) direction generated by relativistic electron beams with energy up to 100 MeV and rectangular perfectly conducting gratings are presented. The results obtained prove the equivalence of the Smith-Purcell radiation field in both cases of propagation for the electron beam.
Helical radial sinusoidal modulated wiggler
V. I. R. Niculescu, Vasile D. Babin, Mihaela Dan
A new theoretical model of a wiggler for free electron lasers in an altered helical magnetic field is presented. The wiggler is a helicoidal widding having a simultaneous radial sinusoidal modulation. Analytical approximate expressions of the magnetic field components using multiquadratic basis functions were obtained. This new treatment of the problem could be extended to the nonlinear dinamical analysis of the electrons in the studied structure.
Rate equations for an erbium laser system: a numerical approach
Florin C. Maciuc, Costin I. Stere, Andreea-Rodica P. Sterian
In our work, we develop a numerical model for studding the variation of phenomenological and optical parameters in an Er+3 system of 6 excited levels that is subject to a lasing condition. The model is using a four order Runge- Kutta method to solve a system of eight time-dependent variables. The simulations, based on the change of pumping wavelength, prove that the highest efficiency is reached for a 970 nm pump wavelength, concordant with the existing literature results. Different processes, including: three ion-ion up-conversion processes, two pumping processes and the inherent spontaneous transition, are considered.
Lasers in Material Sciences
icon_mobile_dropdown
Fundamental aspects of photochemical effects in UV laser ablation
Athanasia Athannassiou, D. Fragouli, Efi Andreou, et al.
The photochemical effects induced by UV irradiation at 248 nm to highly photosensitive organic compounds embedded into polymer matrices are sutdied in a systematic way using laser induced fluorescence. The nature and intensity of the induced photoproducts are monitored below and above the ablation threshold. Host polymers with different absorption coefficients in the employed wavelength are used in order to study their protective role with regard to the photodissociation of the dopants. The employed dopants are the iodo-derivatives of naphthalene and phenanthrene (NapI and PhenI). Photolysis of the dopants, while they are embedded int he weakly absorbing polymer PMMA, at laser fluences below the ablation threshold is found to result in the formation of naphthalene-like and phenanthrene-like photoproducts, whereas above the threshold, additional photoproducts are clearly observed only in the case of the NapI dopant. The photolysis yields for both dopants exhibit very similar behaviour, increasing sharply above the threshold. In contrast, in the case where the dopants are embedded into the strongly absorbing polymer polystyrene, their photolysis yields reach a limiting value closely above the ablation threshold. Therefore, the absorbing polymer provides a high degree of control over the induced photochemical effects. The finding implies that the photolysis efficiency of the incorporated additives is directly affected by the host polymeric material.
Holographic interferometry sequential investigation of long-term photomechanical effects in the excimer laser restoration of artworks
Vivi Tornari, Antonia Bonarou, Vassilis Zafiropulos, et al.
Excimer laser ablation utilized in artwork restoration generates pressure waves that may influence the structural integrity. By means of holographic interferometry a non- destructive highly sensitive mapping for evaluating the structural state is provided. The long-term sequential recording enables comparison between time resolved optical wave fronts scattered from the artwork before and after the selective ablation of material. Thus, comparative structural monitoring of laser-induced photomechanical effects that may result in potential damage of the artwork is accomplished.
Ferroelectric thin films deposited by pulsed laser deposition
Raluca Dinu, I. Vrejoiu, P. Verardi, et al.
Influence of substrate and electrode on the properties of PbZr0.53Ti0.47O3 (PZT) thin films grown by pulsed laser deposition technique (1060 nm wavelength Nd:YAG laser light, 10 ns pulse duration, 10 Hz repetition rate, 0.35 J/pulse, 25 J/cm2 laser fluence, deposition rate about 1 angstrom/pulse) was studied. The substrate temperatures were in the range 380 degree(s)C-400 degree(s)C. Oriented crystalline PZT layers with 1-3 micrometers thickness were deposited on glass substrates plated with Au/Pt/NiCr electrodes, from a PZT commercial target in oxygen reactive atmosphere. The deposited PZT films with perovskite structure were preferentially oriented along the (111) direction as revealed from XRD spectra. Piezoelectric d33 coefficients up to 30 pC/N were obtained on as deposited films. Ferroelectric hysteresis loops at 100 Hz revealed a remanent polarization of 15 (mu) C/cm2 and a coercive field of 100 kV/cm. A comparison with properties of PZT films deposited using a KrF laser and with SrBi2Ta2O9 (SBT) films is reported.
Synthesis and characterization of iron clusters coated with hydrocarbons
Friedrich Huisken, Bernhard Kohn, Rodica Alexandrescu, et al.
Iron clusters were produced by CO2-laser-induced decomposition of iron pentacarbonyl in a flow reactor using SF6 as a sensitizer. By adding hydrocarbon molecules (e.g. C2H4), which were also dissociated in the laser field, the iron clusters were allowed to react with several radicals. The as-synthesized species were extracted from the reaction zone by a conical nozzle and expanded into the source chamber of a cluster beam apparatus where they were analyzed with a time-of-flight mass spectrometer. At sufficiently high C2H4 concentration, we observed the appearance of a magic peak in the mass spectrum at mass m equals 884 amu. Using C2D4 instead of C2H4, the magic peak shifted by 12 amu to larger masses, indicating that the magic cluster must contain 12 hydrogen atoms. With the given restrictions, we readily derive the sum formula Fe13C12H12. Chemical stability and symmetry considerations suggest that the detailed chemical formula of the magic cluster is Fe13(C2H26 or Fe13(CequalsCH2)6 and that its structure corresponds to a Fe13 icosahedron with six HCequalsCH or CequalsCH2 groups bound to six pairs of the 12 iron surface atoms.
Oxidized porous silicon waveguides losses
G. Lamedica, M. Balucani, V. Bondarenko, et al.
The Oxidized Porous Silicon Waveguides (OPSWG) present the chance to realize waveguide in the visible range compatible with integrated circuit (IC) fabrication technology. In OPSWG the light is confined in dense silica surrounded by a buffer of porous oxidized silicon. In this paper some of the results of the European project OLSI N degree(s) 28.934 are discussed. The waveguides were fabricated using p-doped (100) and n-doped (100) and (111) silicon wafers to investigate the influence of the doping type and of silicon crystal orientation on the guiding properties and the thickness of the buffer layer was varied from 1 micrometers to 2.5 micrometers changing the anodization regimes and the propagation losses were measured. Two different topology of mask have been used to determine propagation and planar bending losses. Buried OPSWG, realized depositing one micron poly- silicon layer on top of waveguides, have been thermally treated and measurements have not shown a great difference in terms of propagation losses with surface OPSWG.
Laser ablation of aged resin layers: a means of uncovering the scalar degree of aging
Vassilis Zafiropulos, Alexandra Manousaki, Agathi Kaminari, et al.
This is the first study on the scalar properties of an aged resin film. The present work is concentrated in using the laser ablation as a means of studying the scalar characteristics of various spectral properties that are related to the degree of aging. It is shown that the observed trend has an exponential dependence on the distance from the surface, which in turn is associated with the exponential intensity distribution of UV light within the film. The results open the way of understanding the oxidation and polymerization mechanisms from a cross sectional point of view in the resin film.
Pulsed laser deposition of thin films for optics applications
M. L. De Giorgi, M. Fernandez, Gilberto Leggieri, et al.
SiO2 and ITO (indium tin oxide) were deposited by ablating Si, SiO and ITO targets, respectively, in low- pressure oxygen atmosphere with pulsed XeCl and KrF excimer laser. The SiO2 and ITO films were deposited on Si<100> and glass (BK7) substrates at temperatures of 20-600 degree(s)C. The substrates were generally set parallel to the target. To reduce droplet deposition in SiO2 films, the off-axis configuration or the so-called eclipse method, characterized by a shadow mask between target and substrate were used. Dense, continuous ITO films with resistivity as low as 1.6x10-4/ (Omega cm and a high transparency (80-90%) in the visible and near-infrared regions were deposited. Ultra-thin (approximately 6 nm) films were deposited and successfully used as electrodes in optoelectronic devices. Dense, stoichiometric, thick (>2 micrometers ) SiO2 films were deposited on substrates either at room temperature or heated at moderate temperatures (100- 600 degree(s)C). Droplet density and surface roughness strongly depend on ablation configuration. Roughness can be kept quite low (approximately 5 nm) by using the KrF laser and a quite large target-to-substrate distance (8-12 cm). It is shown that multi-component films like ITO and Silica (SiO2) can be efficiently deposited by using the reactive pulsed laser deposition technique.
Fullerene/iron complexes obtained by laser synthesis from gas/aerosol phases
Rodica Alexandrescu, Aurelian Crunteanu, Ion G. Morjan, et al.
The preliminary results on the laser synthesis of carbonaceous nanoparticles, which exhibit some characteristic features of fullerene/iron complexes, are reported. The nanopowders were obtained by the laser pyrolysis of a gas phase mixture containing hydrocarbon and alternatively iron pentacarbonyl vapors or ferrocene aerosols. The vapors of iron pentacarbonyl were carried out in the reactor through the intermediate of a bubblier; in the runs using ferrocene, this one was solved in benzene and brought into the reaction zone as aerosol. The reactant mixture contained also nitrous oxide, as oxidizer, and sulphur hexafluoride as energy transfer agent. The as- synthesized powders were toluene extracted and characterized by different analytical methods, such as High Performance Liquid Chromatography (HPLC), IR transmission spectroscopy and Moessbauer spectroscopy. The identification of fullerene-metal complexes was performed by Moessbauer spectroscopy. The Moessbauer transmission spectrum has evidenced the formation of both fullerene phases with iron inside and outside the cage.
Ultraviolet-assisted pulsed laser deposition: a new technique for the growth of thin oxide films at medium and low temperatures
Valentin Craciun, Doina Craciun, Joshua M. Howard, et al.
The crystallinity, stoichiometry and optical and electrical properties of thin Y2O3, ZnO and Ba0.5Sr0.5TiO3 films grown using an in situ ultraviolet (UV)- assisted pulsed laser deposition (UVPLD) technique have been studied. With respect to films grown by conventional PLD under similar conditions but without UV illumination, the UVPLD grown films exhibited better quality, especially for lower substrate temperatures. They also contained less physisorbed oxygen than the conventional PLD grown layers. These improvements can be explained by the action of several factors. Firstly, deep UV photons and ozone ensure a better in situ cleaning of the substrate. Secondly, the presence during the ablation-growth process of more reactive gaseous species like ozone and atomic oxygen formed by photodissociation of molecular O2 promotes the oxygenation of the films. Thirdly, absorption of UV photons by adatoms could result in an increased surface mobility. All these factors have a beneficial effect upon crystalline growth, especially for moderate substrate temperatures, where the thermal energy available for the process is rather limited.
Synthesis of nanosized aluminum nitride powders produced by laser ablation
Constantin Grigoriu, Makoto Hirai, Weihua Jiang, et al.
We have investigated the influence of the laser fluence, ambient nitrogen and target material on the synthesis of aluminum nitride nanosized powders by reactive laser ablation. Pure aluminum and aluminum nitride were used as targets. The study revealed that were pure nanosized AlN powders (3-25 nm in diameter) can be synthesized for laser fluences higher than 11 J/cm2(approximately 1.6 GW/cm2). AlN powders were obtained at any nitrogen pressure in case of AlN target, while aluminum target pressure >= 100 Torr was required.
Experimental study of the interaction of intense electron beams with metallic targets
Mircea V. Udrea, Mihaela Stoica, Mihai Ganciu, et al.
Preliminary studies regarding the interaction of intense short electron beams with different metallic targets are presented. The electron generator consists of a fast filamentary discharge in low-pressure gases. The filling gas is Helium, Argo, or Nitrogen at approximately 0.1 Torr pressure. The target might be easily changed. Also, the beam might be magnetically deflected in order to be properly directed. The interaction of the beam with different targets was investigated by means of a scanning electron microscope. The device is capable to drill holes of several tenths of microns in diameter in metallic targets.
Ablation study with a Nd:YAG laser in enhanced free-running regime
The research is carried on as a project in the frame of the PHARE-TTQM program, a cooperation of INFLPR Bucharest, PRO OPTICA SA Bucharest and FORTH-IESL Heraklion-Greece. A new laser ablation technique, based on the enhanced free running (EFR) mode of operation of a Nd:YAG laser, is presented. In the EFR degree(s) mode it is possible to achieve a regular temporal structure of the laser spiking combined with the control of both amplitude and separation of the individual spikes. The stable fluence and power density of the spikes will increase the precision of the EFR laser ablation in comparison with the short free running technique. The short duration of the EFR spikes, combined with their large time separation, reduces the level of the thermal damage of the substrate. A surface processing laser device operating in EFR mode is under development with PHARE financial support in the Laser Department of INFLPR. Preliminary study of ablation of stone samples from Stavropoleos Monastery, Bucharest, using FORTH-IESL laser facilities, is presented.
Simplified model for RMS variation in pulsed laser deposition
In Pulsed Laser Deposition (PLD) surface roughness of a deposited film is an important parameter for many thin films applications. Plume free expansion and propagation in a plane shadow mask experimental setup have been investigated together with film roughness for several deposition parameters. In this paper we propose a simplified formula for a RMS variation. A comparison between theoretical and experimental results is presented. The model is considered to be useful for quick roughness (RMS) estimation in PLD deposition.
Hydroxyapatite thin films growth by pulsed laser deposition: effects of the Ti alloys substrate passivation on the film properties by the insertion of a TiN buffer layer
Valentin D. Nelea, Carmen Ristoscu, Cornel Ghica, et al.
Hydroxyapatite (HA), Ca5(PO4)3OH, is now widely used in stomatology and orthopedic surgery. Due to a good biocompatibility combined favorable bioactivity make as HA to be considered as a challenge to successful bone repair. We grow HA thin films on Ti-5Al-2.5Fe alloy substrate by pulsed laser deposition (PLD) technique. The films were deposited in vacuum at room temperature using a KrF excimer laser ((lambda) equals 248 nm, (tau) FWHM >= 20 ns). After deposition the HA films were annealed at 550 degree(s)C in ambient air. The insertion of a bioinert TiN buffer layer at the HA film-metallic substrate interface was studied in terms of HA film microstructure and mechanical properties. SEM, TEM and SAED analysis structurally characterized films. The mechanical properties were evaluated by nanoindentation tests in static and scratch modes. Films with TiN interlayer contain uniquely crystalline HA phase and present better mechanical characteristics as compared with those deposited directly on Ti-alloy substrate.
Laser surface treatment of materials by using CO2 laser beam at oblique incidence
M. Taca, E. Alexandrescu, V. Fantini, et al.
The amount of the heat transferred to the workpiece is of high importance on the laser surface treatment. A possibility to increase the energy coupling efficiency by using oblique incidence of the laser beam is proposed. The drawback of oblique incidence technique consists in the deformation of the laser intensity profile on the irradiated surface at large incidence angles (70-80 degrees). This paper is dealing with a method to overcome this disadvantage: focusing the laser beam in an elliptical shape at normal incidence; using oblique incidence at large angles (70-80 degrees) a circular focused p-polarized spot is obtained. The absorption is (2.5-4) times enhanced and the focused spot on the surface has a circular shape. The use of oblique incidence of the laser beam allows another important advantage: the avoidance of the contamination of the focusing optics. The cladding experiments at 75-degree incidence angle have been carried out at only 650 W laser power level. An improved cladding efficiency was obtained.
CNx films deposited using combined deposition method: pulsed laser deposition in the RF discharged nitrogen gas
J. Bulir, Miroslav Jelinek, Jan Lancok, et al.
Thin CNx films were deposited by pulsed laser deposition (KrF excimer laser) with additional radio-frequency discharge of the nitrogen gas. Nitrogen pressure was in the range from 1 to 40 Pa and r.f. power was adjusted to 100 W. The substrate temperature was changed in the range from room temperature to 800 degree(s)C. An influence of the substrate temperature on the film composition and structure was studied. The composition of the films was measured by wavelength dispersive x-ray spectroscopy. The N/C ratio of films deposited at room temperature almost reach 1; however, it decreased with increasing substrate temperature. Structure was studied using Fourier transformed infrared spectroscopy analysis. Presence of CequalsC, CequalsN, CequalsVN, N-H and O-H groups was confirmed. Optical properties were analyzed using UV-VIS reflection spectroscopy.
Thin films CdTe/CdS heterostructures 2: chemical-bath-deposited cadmium sulphide layers
Ligia Pascu, Elisabeth-Jeanne Popovici, Crina Dan, et al.
CdTe/CdS heterojunctions are valuable candidates for photovoltaic conversion of solar energy. Cadmium sulphide thin layers have been glass deposited from chemical bath containing cadmium acetate, thioureea, sodium citrate and ammonia. The CdS/glass structures were characterized by UV- VIS reflectance and transmittance spectroscopy and x-ray diffraction spectroscopy; the microstructural parameters of CdS films were determined by single x-ray profile. The influence of the deposition procedure, i.e. in monolayered and multilayered form as well as that of the post-growth thermal treatment on the optical and structural properties of CdS films was studied.
Monte Carlo simulation of transit of ablated atoms through ambient gas
Johny Neamtu, Ion N. Mihailescu, Carmen Ristoscu
We made a Monte Carlo simulation of the elastic interaction of ablated atoms with ambient gas molecules. Varying the initial energy of ablated atoms, the simulations were performed for different values of the ambient gas pressure in the range of 0.1-100 Pa and/or for values of target collector distance between 3-7 cm. The results concern the Ti ablated atoms transit in methane. Calculating the energy of the atoms when they reach the collector we determine the condition for plume splitting occurrence.
Absorption mechanisms in UV laser plasma
Johny Neamtu, Ion N. Mihailescu
We report a theoretical study of the integration between UV laser pulse and the plasma expanding in front of the target. For description of the laser-plasma interaction process we used the gasdynamic approach. The plasma is assumed to be an electrically neutral gas, which contains neutral atoms, ions, and electrons in Local Thermodynamic Equilibrium (LTE). For study this interaction we used an Coupled Euler Lagrange numerical code. In addition it was possible to investigate the mechanism of plasma absorptivity and also calculating the laser energy which is effectively transmitted to the target.
Low-temperature growth of high-quality indium tin oxide thin films by ultraviolet-assisted pulsed laser deposition
Valentin Craciun, Doina Craciun, Z. Chen, et al.
Indium tin oxide (ITO) films were grown on (100) Si and Corning glass substrates by an in situ ultraviolet-assisted pulsed laser deposition (UVPLD) technique. The most important deposition parameter for the growth of high transparent and conductive ITO films was found to be the oxygen pressure used during the deposition. Films grown under low oxygen pressure were brown and exhibited low optical transmittance and high resistivity. For a target- substrate distance of 10.5 cm, which ensured a uniform film across 2.5 cm, the optimum oxygen pressure to obtain the lowest electrical resistivity was found to be around 10 mTorr. For higher oxygen pressures, the optical transmittance was a little bit higher but a significant increase of the electrical resistivity was noticed. X-ray photoelectron spectroscopy showed that ITO films grown in the 5-20 mTorr range were fully oxidized, without any measurable metallic content. Films grown at room temperature were amorphous regardless of the oxygen pressure used.
Removal of the indigo color by laser beam-denim interaction
Traian Dascalu, Sofia E. Acosta-Ortiz, Martin Ortiz-Morales, et al.
We proved in our experiments that the laser fading process removes efficiently indigo-dye from denim support. Different laser pulse parameters were used in order to obtain laser power density and fluence to start the ablation process. The purpose of this work is to determine the change of denim diffuse reflectivity spectra during laser irradiation with different wavelength and different power density. The change of diffuse reflectivity coefficient was up to 17% at 450 nm wavelength (from 8% reflectivity for unirradiated denim). We use the beams from Nd:YAG laser (1064 nm and its second harmonic 532 nm) and CO2 lasers.
Synthesis of manganese-activated zinc silicate phosphor
Elisabeth-Jeanne Popovici, Laura Ungur, Cristina Ciocan, et al.
Manganese activated zinc silicate is a classical phosphor with large applications in optoelectronic device manufacture. Some aspects concerning the influence of precursor quality on Zn2SiO4:Mn phosphor formation and properties are presented. Phosphor samples were prepared by classical ceramic technique from homogeneous mixtures consisting from MnCO3 and various sorts of SiO2 and ZnO sources. The precursors and phosphor characterization was achieved by thermal analysis, surface area measurements, IR spectroscopy, x-ray diffraction and fluorescence spectroscopy. The quality and reactivity of precursors influence Zn2SiO4:Mn phosphor formation rate thus conducting to materials with different structural and luminescence characteristics.
Synthesis of europium- or terbium-activated calcium tungstate phosphors
Flavia Forgaciu, Elisabeth-Jeanne Popovici, Laura Ungur, et al.
Utilization of luminescent substances in various optoelectronic devices depends on their luminescent properties and sensitivity to various excitation radiation as well as on particle size distribution and crystalline structure of luminous powders. Calcium tungstate phosphors are well excited with roentgen radiation, so that they are largely used for manufacture of x-ray intensifying screens. Being sensitive to short UV-radiation as well, they could be utilized in Plasma Display Panels or in advertising signs fluorescent tubes. In order to diversify the utilization possibilities of this tungstate class, luminescent powders based on CaWO4:Eu3+ and CaWO4:Tb3+ were synthesized and characterized. As compared with the starting self-activated phosphor, larger excitation wavelength domain and emission colors from blue-to-green-to- yellow-to-red were obtained. The good UV excitability and variable luminescence color recommend these phosphors for optoelectronic device manufacture.
Reactive pulsed laser deposition of InN thin films
Raluca Elena Morjan, Alessio Perrone, A. Zocco, et al.
III-V nitrides group are promising materials for technological applications such as: semiconductor lasers, light emitting diodes, optical detectors and refractory materials. In addition, transistors based on the group III nitrides should operate at higher temperatures and under more adverse conditions than similar devices on silicon, II- VI materials, or other III-V materials, due to the high band gap, the strong chemical bonds and the high chemical inertness of the nitrides. The paper reports the first results concerning the deposition of InN thin films by reactive laser ablation of indium target in nitrogen atmosphere. A XeCl excimer laser ((lambda) equals308 nm, (tau) equals30 ns) was used as laser source. The laser beam was incident on the target with an angle of 45 degrees, laser fluency was set at 5 J/cm2. In order to achieve uniform irradiation condition and to avoid fast drilling, the target was rotated with 180 rpm. KBr, Si and sapphire substrates were positioned at 3.5 cm from the target and parallel to it. The nitrogen pressure during deposition was set at 1*10-4, 5*10-3 and 5*10-1 mbar, respectively. Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDAX), and X-ray Diffraction (XRD) analysis were carried out in order to check the composition, structure and the surface aspect of the deposited layers.
Chromatic analysis of the pigments behavior after laser irradiation
Roxana N. Radvan, Nicoleta Popescu, Suzana Dan, et al.
Paper presents a study on the chromatic stability of the pigments and colors with certain mediums after a controlled laser irradiation (1064 nm). The present paper contains observations and conclusions about Nd:YAG laser limits of application on artwork polychromatic surface in concordance with laser beam parameters and colors composition. Main qualitative comments are based on reflection spectral measurements and trichromatic diagrams X, Y, Z in concordance with international norms CIE 1976 (CIELAB). Chromatic coordinates and color variations are calculated.
Working distance control and aiming system for artwork restoration equipment with laser beam
Roxana N. Radvan, Roxana Savastru, Dan Savastru
Work is oriented towards opto-mechanical constructive solutions with high precision for complex microscope equipment with laser for artwork restoration. An important part of the restoration protocols applied in different area of art restoration/conservation requests microscopic investigation and double operation decision - automatic and manual operation. Working distance control and its adjustment represents the main difficulty for automatic laser cleaning process. On the other hand, IR or UV laser spot have to be marked by a visible beam and to support user decision increasing the equipment accuracy. Paper presents the optical arrangement of a laser microscope for artwork, investigation and cleaning with an optical system of aiming and metrological principle of working distance control.
Whiteness behavior of artwork's various materials after cleaning process using Nd:YAG laser beam
Roxana N. Radvan, Nicoleta Popescu, Suzana Dan, et al.
This paper presents some studies for evaluating laser treatment/cleaning of white materials - grounds and papers. The results of the induced modifications of the whiteness of some irradiated samples in a controlled procedure are analyzed. The task of this study is the determination of the Nd:YAG laser optimum-working regime for cleaning applications.
Synthesis of cerium-activated strontium-magnesium orthophosphate phosphors
Maria Vadan, Elisabeth-Jeanne Popovici, Laura Ungur, et al.
Cerium activated strontium-magnesium orthophosphate phosphors could be used in the manufacture of erithermal or copy machine lamps. Under short wave UV radiation, cerium activated strontium-magnesium orthophosphate exhibits strong UV luminescence with emission maximum at 370-380 nm. The luminescent emission depends on both host matrix composition and activator amount. Samples of (Formula available in paper):Ce phosphors with variable composition, i.e., different Mg/Sr ratio and variable cerium content, were synthesized and characterized in order to establish the optimum host lattice composition and cerium concentration.
Nonlinear, Quantum and Information Optics
icon_mobile_dropdown
Novel optical microscopy
Norbert Kroo
Near field microscopy has proved to be an efficient tool to break the Rayleigh criterion of resolution. A high spatial frequency object generates evanescent waves if illuminated by propagating or evanescent waves. The generated, non- detectable local field may partly be turned into a propagating wave by a small scatterer, which can already be detected, reflecting the spatial structure of the object. This principle is used in different forms in sub-wavelength resolution microscopy down to the nanometer scale. If the scatterer is the tip of a scanning tunneling microscope (STM), the evanescent field-tip interaction leads to the change of the tunneling current, resulting in a special type of the near field microscope. The evanescent field could be that of surface plasmon oscillations (SPO). The state of art of near field microscopy, and as an example the SPO-STM case, is discussed in detail.
Spectroscopy with single-trapped ions
Herbert Walther
In this paper experiments with single trapped ions are reviewed. They are performed with the aim of developing a new frequency standard and to perform cavity quantum electrodynamics experiments with single ions. For a new optical frequency standard we are investigating the 5s21S0 implied by 5s5p3P0 transition of a single trapped laser-cooled 115In(superscript + ion. This line with a natural linewidth of only 0.8 Hz is highly immune to systematic frequency shifts. For sideband laser cooling and fluorescence detection of the indium ion the 5s21S0 implied by 5s5p3P1 transition at 230.6 nm is used. Temperatures below 100 (mu) K and a mean vibrational quantum number <n><1 of the ion in the trap have been reached. For the clock transition a resolution of 1.3 multiplied by 10-13 (linewidth 170 Hz) has been obtained so far, limited by the short term frequency fluctuations of the clock laser. The absolute frequency of the 1S0 implied by 3P0 transition was measured by making a link to the reference frequency of the methane-stabilized HeNe laser using a frequency chain. In the second part of the paper the present status of the experiments on the ion trap laser are briefly described.
Speckle revisited: analysis of speckle noise in bar-code scanning systems
Emanuel Marom, Sasa Kresic-Juric, Leonard Bergstein
Laser beams used for bar-code scanning exhibit speckle noise generated by the roughness of the surface on which bar-codes are printed. Statistical properties of a photodetector signal that integrates a time-varying speckle pattern falling on its aperture are analyzed in detail. We derive simple closed form expressions for the auto-correlation function and power spectral density of the detector current for general form scanning beams with arbitrary field distributions. Theoretical calculations are illustrated by numerical simulations.
Optical properties of As2S3 and As2Se3 glasses doped with Dy, Sm, and Mn
Andrei M. Andriesh, Mihai S. Iovu, Sergiu D. Shutov, et al.
The effect of low amounts of dysprosium, samarium and manganese (0.1-0.5 at.%) on structure and optical properties of chalcogenide glassy semiconductors As2S3 and As2Se3 is investigated. The fundamental absorption edge shifts to longer wavelength with doping; the largest shift was observed for As2S3 glasses doped with Dy and Mn. A correlation of the properties with medium range order and electronegativity of impurity atoms was revealed. Photodarkening relaxation under light exposure of a-As2Se3 amorphous films doped with 0.5 at.% of metals Sn, Mn, Sm and Dy was studied in dependence on the impurity and thermal treating. Both factors reduce photodarkening and the degree of reduction depends on the sort of impurity. The relaxation process may be described by a stretched exponential with the dispersive parameter 0.5
Development of a 10-Gbit/s optical soliton source
Paulo S. Andre, Armando H.M. Nolasco Pinto, Joao Lemos Pinto, et al.
In this work we demonstrated the feasibility of a 10 Gbit/s optical soliton source based on direct modulation of a semiconductor laser. We also show that it is possible to reduce substantially the frequency chirp, induced by the direct modulation process, with a narrow optical filter. A peak power greater than 100 mW is achieved with an optical signal-to-noise ratio (OSNR) better than 39 dB. We measured the output timing jitter of the source and we show that its main contribution is due to the laser noise. We successfully test our source in a 45-km 5-channel WDM system. The stability and easy assembly of this type of source make them attractive for upgrading single or multichannel chromatic dispersion limited optical communication systems.
Characterization of upconversion phenomena in Er3+-doped Ti:LiNbO3 waveguides using the fluorescence around 550 nm
Niculae N. Puscas, Bruno Wacogne, Vincent Voinot, et al.
In this paper, we report theoretical and experimental results concerning the upconversion phenomena around 550 nm in Er3+-doped Ti:LiNbO3 waveguides. This phenomena corresponds transitions between the levels 4S3/2 implied by 4I15/2. The waveguide is pumped near 980 nm with a laser diode. Two pump photons are used to bring the Er ions to the short lifetime level 4F7/2. After a non-radiative transition to the level 4S3/2, Er ions emit photons at 550 nm while falling down to the 4I15/2 level. By using the theoretical model elaborated by McCumber we evaluate the homogeneous emission cross sections and we obtain the following maximum values of the cross sections (sigma) He(551.9 nm) equals 57.7 x 10-26 m2 for TE and (sigma) He(558.1 nm) equals 52.5 x 10-26 m2 for TM polarizations. By measuring the fluorescence radiation around (lambda) equals 550 nm, we determine the rising and falling times and we obtain C equals 0.198 x 10-23 m3/s as the value of the modulus of the homogeneous upconversion factor the value. The results presented here can be used in the design of integrated optoelectronic circuits and in the modeling of the laser action and optical amplification in Er3+-doped Ti:LiNbO3 waveguides when a 980 nm pumping is considered.
Experimental demonstration of (1+1)D self-confinement and breathing of laser beams in BSO crystals
Eugenio Fazio, F. Mariani, Mario Bertolotti, et al.
We report the experimental observation of (1+1)D self- confinement of laser beams in BSO crystals, photorefractive materials with strong optical activity (45 degree(s)/mm). Numerical simulations of light propagation in such conditions were used to check the experimental results. The possibility of obtaining self-contained beams with these materials is given by the application of really intense static electric fields which induce anomalous behaviour of the optical activity.
(2+1)D spatial solitons in photorefractive crystals with strong optical activity and absorption
Valentin I. Vlad, V. Babin, Mario Bertolotti, et al.
We demonstrate the generation of solitons in the photorefractive materials with strong optical activity and absorption. The general wave equations are processed by rotation and affine transformations in order to decouple the effects of photorefractivity and optical activity. Analytical solutions of these equations are found in the case of slowly varying envelope and low-intensity approximations. The solutions show the occurrence of breathing solitons in sillenite crystals with strong optical activity and absorption in a particular orientation with respect to the external electric field. The absorption is decreasing the soliton intensity with the propagation distance (which set a limit in the soliton channel length) and is increasing the breathing period.
Quantum communication and single-photon technologies
Anders Karlsson, Mohamed Bourennane, D. Ljunggren, et al.
We discuss single-photon counting technologies, in particular at the optical wavelength of 1550 nm and their application in quantum communication. In particular we discuss the case of quantum cryptography illustrating with experiments performed in our lab, supplemented by recent experiments by other groups. We furthermore discuss briefly more general protocols for quantum communication and address some experimental changes.
Optoelectronic implementation of cellular automata for complex vision algorithms
Pierre H. Chavel, Alvaro Cassinelli, I. Glaser
In this work, we elaborate on the compromise between the efficiency of the multiprocessor computer architecture for handling large classes of computing tasks and the good performance of optics for implementing shift invariant operations, in particular convolution. We derive a class of processors, optoelectronic cellular automata that can efficiently implement intensive, low level vision tasks in a time compatible with application constraints up to standard video rates. As one illustration, a parallel simulated annealing task performing motion detection on an image sequence is demonstrated.
Optical spatiotemporal solitons in quadratic media
Dumitru Mihalache, Lucian-Cornel Crasovan
Numerical studies of the propagation of ultrashort optical pulses in quadratic nonlinear media are presented. Two- parameter families of chirped stationary spatiotemporal solitons in dispersive quadratically nonlinear media are constructed in the presence of temporal walkoff. It is found that the walking spatiotemporal solitons are dynamically stable in most cases. We find also one-parameter families of spinning spatiotemporal bright solitons in dispersive media with quadratic nonlinearities and study their stability. The comparison with a simple variational approximation for the spinning spatiotemporal solitons demonstrates that, though the variational approximation is not very accurate, it correctly describes the qualitative features of the spinning spatiotemporal solitons. We show that the spinning spatiotemporal solitons are subject to a storing azimuthal instability. The instability breaks the spinning soliton into stable nonspinning light bullets.
Multiwave mixing in anharmonic photorefractive thin gratings with modulation close to unity
Adrian Petris, Valentin I. Vlad
The high-modulated phase gratings induced in photorefractive crystals are anharmonic. For small angles between incident beams (thin grating regime), an additional mixing can appear between the diffraction orders produced by harmonics of the anharmonic grating. This mixing yields significant changes in the self-diffraction spectra. Our theoretical and experimental results explain the effect of the grating anharmonicity on the self-diffraction on thin photorefractive gratings.
Modeling the optical gain and noise in the bent Er3+-doped LiNbO3 waveguide of the Mach-Zehnder interferometer
Niculae N. Puscas, Adrian N. Ducariu, Lucian Ene
Er3+-doped LiNbO3 is widely used for the fabrication of integrated optic components. In the small gain approximation and the unsaturated regime in this paper we report some original results in the evaluation of the spectral optical gain and spectral noise figure in the bent Er3+-doped LiNbO3 waveguide of the Mach-Zehnder interferometer pumped near 1484 nm using erfc, Gaussian and constant profile of the Er3+ ions in LiNbO3 crystal. We used a quasi-two-level model to simulate the optical amplification in Er3+-doped LiNbO3 straight and bent waveguide amplifiers and we demonstrated that rather high gains (similar to 1.1 dB) and low noise figures (similar to 3.3 dB) at the end of the bent arm of the Mach-Zehnder interferometer are achievable for 100 mW input pump power. The obtained results can be used for the design of the integrated Mach-Zehnder interferometers and optic devices.
Optical fibers as high-reflectivity phase conjugate mirrors based on stimulated Brillouin scattering
Anca Mocofanescu, Oliver Mehl, Hans Joachim Eichler
Phase conjugate mirrors based on stimulated Brillouin scattering (SBS) in multimode undoped quartz fibers can be operated with high reflectivity. The reflectivity and threshold of the SBS process and the damage threshold of the fiber entrance surface were measured for fibers with core diameter of 25, 50, 100, 200 micrometers . With calibration of the measurement system such fibers can operate with more than 80% reflectivity and the damage threshold lies above 0.9 GW/cm2. The SBS threshold is between 0.3 and 26 kW for all fibers investigated.
Electrical and transport characteristics of doped Bi12TiO20 photorefractive single crystals
Bi12TiO20 single crystals doped with Cd, Cu, P, Cr, Ag, Al were grown by the top-seeded solution growth method (TSSG). The electrical measurements were carried out on different BTO samples. The electrical conductivity followed the Arrhenius low, with an activation energy ranged from 0.38 to 0.63 eV. Mobility and transport properties of charge photo carriers were investigated by the time-of-flight technique. For non-doped BTO and doped with Cu, P, Al and Cd the obtained values for drift mobility of electrons varying between (mu) equals10-2 and 1 [cm2/V.s]. In the case of BTO doped with Al the dominant charge carriers were holes with mobility (mu) equals5x10-3 [cm2/V.s]. These key photorefractive parameters were used to calculate the lifetime of charge carriers using the period of the recorded holographic photorefractive space gratings.
Optical nonlinearities in fatty acids
Mihaela A. Ghelmez, Maria Honciuc, Elena Slavnicu
A variety of self-organized patterns were observed in liquid crystal modulators, generated because of their large and controllable nonlinearity. In this work, we investigated some fatty acids and mixtures with cholesterol, which showed, under certain conditions, thermotropic mesomorphism and a large sensitivity to the optical field. Depending on the transverse profile of the laser beam, a self-phase modulation and external self-focusing - illustrating the nonlinear wave propagation - were observed. A ring pattern, due to the steady-state far-field diffraction intensity distribution of the Gaussian beam of a helium-neon laser, transmitted through the samples, was experimentally and computer studied. This is useful both for building new photonic devices and for explaining some processes from the biological membrane.
Laser beam coherence
Alexandru Popa
In recent papers we presented a wave model for closed conservative bounded systems, whose behavior is described by the Schrodinger equation. For such a system, the Schrodinger equation is equivalent to the wave equation. The analysis of the wave properties reveals an intrinsic coherence of the electron motions. We approximate the fundamental and metastable states of laser active medium by closed conservative bounded systems. We show that the coherence of the laser radiation could be explained by a transition between these coherent states.
Model of selectively buried optical waveguides
Alexandru I. Lupascu, Dominique Persegol
Selective buried waveguides have different regions, lying at various depths under the glass surface. This structure is formed by field-assisted inter-diffusion in an electrically inhomogeneous glass, with an electrical conductivity varying both spatially and in time. We present a simple, preliminary model of such a complex, two-dimensional structure. We explain the assumptions used to obtain a tractable model and discuss them in detail. Our results are illustrated by mono- mode structures, buried under normal electric field intensities. They are in qualitative agreement with experimental measurements. We discuss the improvements of the model, necessary to take into account spatial and temporal variations of glass properties.
Fabrication and characterization of Bragg gratings in Er-Yb-doped glass waveguides using interferometric method
In this paper we report some experimental results concerning the fabrication of Bragg gratings with submicronic period in Er-Yb-doped glass waveguides using interferometric method and of a monolithically integrated DFB laser. Also, a method used for monitoring the development process in real time using data acquisition program on a Labview platform and some results related to the characterization of the waveguides with gratings in reflection mode and a monolithically integrated DFB laser pumped at 980 nm are presented and discussed. These results can be used for the improvement of the fabrication processes of the above mentioned devices and optical integrated circuits.
Analysis of the maximum refractive index difference profile of optical waveguides obtained by double ion exchange in glass
Based on some experimental results we report in this paper the modeling of the maximum refractive index difference profile of the optical waveguides obtained in glass by double ion exchange (Ag+) using Gaussian and erfc functions. The dependences of the maximum refractive index difference, the center of the Gaussian and erfc functions in depth and width, respectively and the corresponding variances on the technological parameters: the width of the mask (window), the first and the second in-diffusion time of the ions were evaluated. The simulation results can be used for the analysis and the design of the optical integrated devices.
Analysis of phase-matching conditions for internal second-harmonic generation in InGaAs quantum well laser diodes
M. Frunza, Emil Smeu, Niculae N. Puscas, et al.
In this paper we present an analysis of the phase-matching conditions for internal second-harmonic generation in InGaAs quantum-well laser diodes in order to enhance the conversion efficiency. We have characterized the role of phase- mismatching in the spectral distribution of the internal second-harmonic generation in the CW operation of these lasers. The emission of pairs of narrow blue-green peaks having perfectly symmetrical spectral positions with respect to the central peak of pure second-harmonic generation at approximately 480 nm is most probably enhanced by a mechanism of reciprocal cancellation of the respective phase-mismatch vectors. This study is important for the assessment of the relationship between the structural parameters of the laser and the conditions which contribute to the stimulation of second-order optical nonlinearities in the laser active region.
Analytical treatment of transversal effects in stimulated Brillouin scattering
A three-dimensional wave model for the stimulated Brillouin scattering (SBS) is built and analytically treated, in case of slowly varying envelope approximation and stationary regime. More complete analytical expressions for pump and Stokes wave intensities and for SBS reflectivity are found. A good agreement between theoretical and experimental data for reflectivities is shown for Gaussian transverse profile of the pump beam.
Phenol adsorption using holographic interferometry in photorefractive crystals
Mona Kurzeluk, Anicuta Guzun, Adrian Petris, et al.
Phenol is a major pollutant under strict effluent restriction. Its toxicity is well known, both in aquatic environment and human health. Among the purification technologies, adsorption is widely used in ecological procedures for chemical industry, for water and air purification. In order to check up the adsorbent properties of different adsorbent materials, it is necessary to determine some modeling parameters as the diffusion constants and concentration profiles in the vicinity of the adsorbent. The visualization and measuring method used in this work is double-exposure holographic interferometry using a Bi12TiO20 (BTO) photorefractive crystal (PRC) as reusable recording material and a low cost laser diode, as coherent light source. By holographic methods, we are studying phenol adsorption on granulated active coal and active coal powder. The visualization of the diffusion layer and measurements of its dynamics have been performed.
Visualization and study of heat diffusion in glass by a compact schlieren system
Adrian Petris, Carmen Popa, Dragos Popa, et al.
The experimental study of heat diffusion in glass by a compact schlieren system is presented. The schlieren system has been set up with a single transverse mode laser diode as light source. We have used a plane thermal source (a heated metal plate) to generate thermal fields in a plane glass plate sitting perpendicular to the thermal source. The schlieren images were recorded using a CCD camera and a video recorder connected to a PC. A specific software did a further digital image processing. The experimental results have been checked against a theoretical model of the heat diffusion in an infinite medium at a strong and short thermal excitation by a plane thermal source. A good agreement between experimental and theoretical results was found, up to some differences between the experimental conditions and the theoretical hypotheses, which validate this method as a quantitative one in such experiments.
Polymer-dispersed liquid crystal films using new polymer transformed with coloring matter
Doina Manaila-Maximean, Ana Maria Albu, Boris A. Umanski, et al.
We prepared a copolymer of the maleic anhydride with styrene, to which a colored structure designated for the functionalization was added. The new polymer was used to prepare reverse-mode PDLC films. Reverse-mode PDLC are designed for applications where it is important that the failure of the device is a transparent state, rather than a scattering one. We obtained reverse-mode PDLC using a nematic liquid crystal with negative anisotropy (Delta) (epsilon) <0, LCM 3141 (NIOPIK), and we measured the optical transmission of the film. The system was switched from OFF-transparent state to the ON-scattering one, by a sufficiently small voltage, but with a rather low contrast ratio.
Digital image protection by means of cryptographic mixing transformations
Adriana Vlad, Mihai Petru Mitrea
A lot of research studies have been devoted to image protection, either by cryptographic methods (e.g. Opt. Eng. 35, Sept. 1996) or by watermarking techniques (e.g. Proc. SPIE Vol. 3971). In a previous study, the authors reconsidered and improved the cryptographic mixing transformations proposed by CE Shannon for natural language, obtaining a strong cipher for images, as well. The present paper goes deeply inside of the image protection problem: (1) by presenting some variants for the cryptographic mixing transformations which are good even when burst errors appear in the cryptogram; (2) by enabling the use of an m-gram substitution in the mixing functions; (3) by advancing a bridge between cryptographic methods and watermarking techniques. The illustrations are obtained out of processing: (a) computer-simulated random images obeying different probability laws and autocorrelation functions, (b) natural images, and (c) test images.
Self-consistence criterion for fields reconstruction algorithms
In optical field analysis, like restoration of optical phase from phase-modulated images, data acquisition is the primary step in practical reconstruction algorithm. The relation between the experimental sampling rate and the sampling rate request by a particular algorithm is very important. A prior knowledge of the field characteristics cannot be ever done. In this paper we present a self-consistence criterion, based on Wittaker-Shannon theorem, for fields reconstruction algorithms. The criterion correlate the energy of the output database using primary data acquisition with the energy of a database obtained by sub-sampling initial data and can increase the confidence in the result of a reconstruction algorithm applied to a specific input field. We apply the criterion to validate the phase restoration of a following- pass, inverse cosine transform algorithm.
Laser-thermal diagnostics (LTD) of hidden inhomogeneities in multilayer structures
Leonid L. Fedorenko, Vadym V. Naumov, V. Plakhotny, et al.
The possibilities of the laser-thermal diagnostics of the hidden defects in the solid state materials and multilayer structures are reported. The approach is based on the spectral analysis of the thermal radiation flux induced by the high power pulsed laser-surface interaction. To prove the method, the next things have been studied: (1) the distribution of the temperature and thermal radiation fields in the metal and semiconductor structures that is heated by the pulsed laser radiation under various laser regimes and material parameters; (2) the kinetics of surface and interface charge carriers recombination in the multilayer structures; (3) the thermal emission of the inherent radiation of multilayer structures that determines their basic characteristics: sizes of the macrodefects, thickness of interlayers, depth of penetration, thermal and electric conductivity, rate of heating and cooling of the local areas under the laser beam spot. It was found that even small variation in conditions of the laser-surface interaction due to the metal and dielectric defects and heterogeneity in the material structure can produce large changes in the amplitude and spectra of the laser induced thermal radiation, so such a technique could serve as a powerful tool for noninvasive inspection and express control of the hidden topology in the material structure, and the velocity of the surface carriers recombination of semiconductors can be monitored and controlled well.
Biophotonics
icon_mobile_dropdown
Taking light pressure serious: light as a quasimechanical microtool
Karl-Otto Greulich, Buerk Schaefer, Shamci Monajembashi
Light pressure may arise from absorption and can then be calculated as pressure equals intensity / vacuum velocity of light. Alternatively, it may result from scattering and is then called gradient force. In that case a quality factor Q has to be introduced, which has to be determined by calibration. Its numerical value is between 0.05 and 0.3. By coupling a NdYAG laser into a microscope with a high numerical aperture objective scattering light pressure can be used to move micrometer-sized dielectric objects. Such optical tweezers can be calibrated and have been used to measure forces needed to stretch individual DNA molecules, and to measure forces exerted by the motor proteins myosin, kinesin and dynein non-calibrated optical tweezers are used to handle individual DNA molecules after their coupling to micrometer-sized microbeads. Using enzymes which cut DNA molecules in a sequence specific fingerprint-like pattern, it is possible to analyze DNA on a single molecule basis.
Laser applications in phlebology
Leonardo Longo, S. Mancini, Marco Postiglione
PURPOSE: review of laser used in phlebology METHOD: critical analysis of scientific data taken from the literature and based on 25 years personal experience. RESULTS: we have three groups of laser applications in phlebology: for the diagnosis, as physical therapy and as surgical therapy. DISCUSSION AND CONCLUSION: the laser-doppler studies the microcirculations, the no-surgical therapy shown positive results in the treatment of venous ulcers and for the wound healing. It could be indicate also as antiphlogistic and anti-edema therapy, in superficial thrombophlebitis. The surgical laser is useful for the surgical cleaning of ulcers, for haemorroids, angiomas and telangiectases.
Laser diagnostics in a diesel engine
E. J. van den Boom, P. B. Monkhouse, C. M. I. Spaanjaars, et al.
Results of laser diagnostics inside a 6-cylinder heavy-duty diesel truck engine are presented. Optical access is obtained by quartz windows mounted in the cylinder head and in the piston. The engine is running on commercial diesel fuel, causing strong attenuation of the UV laser radiation. The sprays are visualized by laser induced fluorescence (LIF) from polycyclic aromatic hydrocarbons present in the diesel fuel. The measurements were focused on the formation of nitric oxide that could be detected by LIF as a function of the crank angle. The fluorescence signals were processed in order to obtain relative NO density curves during the combustion process. Evidence was obtained for the formation of NO between rather than within the spray flames.
Self-organizing phenomena induced by LLLT in Henoch-Schoenlein purpura
Laura Ailioaie, C. Ailioaie
Henoch-Schoenlein purpura is characterized by vasculitis of small vessels, particularly those of the skin, gastrointestinal tract, and kidney. Patients have characteristic purpuric skin rash plus all or some of the following: migratory polyarthralgias or polyarthritis, colicky abdominal pain, nephritis. Because until now there is no satisfactory treatment, we applied low level laser therapy (LLLT) in order to compare it with the classical therapy. Twenty-three children (2-15 years of age) have been treated at debut of the disease. They were randomly divided: group A (11 children) received LLLT; group B (12 children) was administrated classical therapy. Two GaAlAs diode lasers (670 nm and 830 nm) were used. The density of energy (4-8 J/cm2), irradiating frequency (2.4 Hz) was applied one session daily, using scanning technique under a special treatment protocol on cutaneous purpuric areas (20 sessions). The best results were obtained in laser group. Despite the complex medication, some patients from group B fell back into the former state after apparent improvement, and two children developed nephritis. The results could be explained by self-organization. LLLT is acting as a trigger factor causing certain systemic effects through circulating blood and a response of the entire immune system, by way of synergetic mechanisms.
Cavity ring down spectroscopy and laser-induced fluorescence for NO2 detection
Angela Staicu, R. Evertsen, N. J. Dam, et al.
The spectroscopic detection of NO2 has been investigated in the visible spectral range by laser induced fluorescence (LIF) and cavity ring down spectroscopy (CRDS). NO2 mixtures with air or argon at different pressures have been studied with LIF by excitation at 532 nm and detection in the range 550-580 nm. Collisional quenching and vibrational energy transfer appear to limit the application of LIF to sub-atmospheric pressures. Therefore, flow samples of NO2 in dry air at atmospheric pressure in the concentration range of 0.1 ppm to 15 ppm have been studied by CRDS. The absorption cross section of NO2 in the range between 437 nm and 450 nm has been determined and compared to literature. The sensitivity of the CRDS system was estimated to be 50 ppb. The effect of elevated temperatures on the absorption coefficient was examined for temperatures of 377 K and 433 K.
v3 band of methane molecule with tunable diode laser absorption spectroscopy
Mourad Zghal, Mokhtar Saidi, Zohra Ben Lakhdar, et al.
Tunable diode laser spectrometers are extensively used for the monitoring of trace gases in the atmosphere. We present the results of experimental researches on atmospheric methane concentration, responsible for industrial pollution in Tunisia. Pulsed and tunable, 3.31 micrometers lead salt, single mode, cryogenically cooled diode laser was employed. Evolution of the laser signal corresponding to methane absorption was observed. The gas to be sampled flows through an optical cell or in open-atmosphere-path. Detection was carried out by observing infrared absorption lines. An acquisition system was developed and data were stored and treated online. Traces of methane at the level of 100 ppb could be detected. This gives access to information involving methane concentration in local atmosphere.
Real efficiency of ambulatory laser treatment at the patients with different rheumatic diseases
Elena-Luminita Sidenco, Sanda Ristache, Luminita Belu
We consulted 189 patients, with different locomotory diseases: degenerative, posttraumatic and chronic inflammatory rheumatic diseases. We followed the main clinical parameters: pain, limitation of mobility, affected function, inflammation and disorders of sensitivity. We applied an infrared LASER source of 100 mW (BTL), daily, for 5 days. The tolerance of the patients at the LASER treatment was excellent (100%). The evolution of the clinical parameters was variated, but inflammation, limitation of mobility and the affected function significantly improved (30-50%). We found a significant diminution of pain (27- 39%). We believe the LASER treatment in ambulatory conditions is essential for the function of the patients with different locomotory diseases.
Porphyrins for photodynamic therapy of cancer
Rodica-Mariana Ion, Mihail-Lucian Pascu
Photodynamic therapy (PDT) of cancer is based on the dye- sensitized photooxidation of different biological targets in the tumoral tissue yielding to a photochemically induced cell's death. The effectiveness of this treatment method depends on the photophysical and photochemical properties of the used photosensitizer-drug during the irradiation with visible light (laser beam) and/or the ionizing radiation. The purpose of this paper is to summarize the photodynamic therapy applications: substitution effects, ionization and aggregation processes effects, photodegradation reaction implications, the correlation with some medical applications on human brain cells.
New method to measure the contraction speed of corneal collagen under laser irradiation
Traian Dascalu, G. Cruz de Leon, M. Consolacion Martinez Saldana, et al.
Laser thermokeratoplasty (LTK) is a very promising method to correct hyperopia and astigmatism. Thermally induced shrinkage of corneal collagen in corneal periphery with IR lasers produce an increasing of central corneal curvature. In order to increase the accuracy of changes in corneal curvature we develop the method to find out the dependence of the collagen's total contraction and contraction speed under laser irradiation. The experiments were performed on porcine eyes, in vitro, by using the fluorescence photobleaching (FP) method and CTH:YAG laser Nd:YAG laser. The collagen fibril was marked with fluorescent collagen antibody. CTH:YAG was used to produce fibril shrinkage and simultaneously an argon laser pulse produce a bleaching pattern on fluorescent marked area. By using the fluorescence microscope the signal detected by a photomultiplier is analyzed and the speed of fluorescent marker and contraction length are detected.
Evidence for benefits of intervention with LLLT in children's asthma
C. Ailioaie, Laura Ailioaie
Asthma is a clinical syndrome characterized by increased responsiveness of the tracheo-bronchial tree to a variety of stimuli. Because of ongoing inflammation even in mild asthmas, we applied as a new modality of treatment, LLLT and a leukotriene antagonist, in order to maximize lung functions and minimize symptomatology in children's asthma. A group of 21 children with mild persistent, moderate or severe asthma were followed for 12 months. The patients were randomly divided into 2 groups. Group 1 (11 patients) received laser therapy combined with Singulair. LLLT was performed with two GaAlAs diode lasers (670 and 830 nm, max output power 50 mW, respectively 300 mW), in cw or pulsed mode using extrameridian acupuncture points and scanning technique, 3 times a week, during 6 weeks. The treatment was repeated after one month-break, for 2 times. Group 2 (10 patients) was administered placebo laser and Singulair, following the same protocol of treatment. The clinical improvement and the immunological characteristics were significantly better in group 1, than in placebo laser group. LLLT and Singulair improve the long-term prognosis and at least partially reverse the natural history of the disease. We strongly recommend it as the most appropriate therapy for asthmatic children.
Laser effects on the growth and photosynthesis process in mustard plants (Sinapis Alba)
Sorin Anghel, Constantin S. Stanescu, Dana Giosanu, et al.
In this paper we present the results of our experiments concerning the influence of the low energy laser (LEL) radiation on the germination, growth and photosyntheses processes in mustard plants (sinapis alba). We used a He-Ne laser ((lambda) equals 632.8 nm, P equals 6 mW) to irradiate the mustard seeds with different exposure times. The seeds were sowed and some determinations (the germination and growth intensity, chlorophyll quantity, and respiration intensity) were made on the plant culture. We ascertained that the germination and growth of the plants are influenced by the irradiation. Also, the chlorophyll quantity is the same for both plants from irradiated and non-irradiated seeds but the respiration and photosynthesis processes are influenced by the irradiation.
Infrared radiometer with digital signal processing for medical applications
G. G. Porumb, Andreea-Rodica P. Sterian, Oana Spulber, et al.
In this paper we present our results concerning the study, design and construction of an infrared radiometer with digital signal processing for medical applications. The design and the practical realization of the system included an a priori study for performing the parameters analysis, both for the radiation source and the detector range, and it can be used for measuring with the desired resolution of the signal power in relation with the diagnosed situations. The pyroelectric type sensor represents the reference element of the system, so that in function of its type and parameters we have designed the source pointing optical ensemble as well as the electronics required for the detector output signal processing. The interface with the operator gives us the possibility of controlling the accuracy of the measurements by using a computer terminal, and also to monitorize the measured values and to modify the parameters by means of an external signal.
Contribution to the spectroscopic study of cytostatics molecules
Angela Staicu, Mihail-Lucian Pascu, Ioan Mogos, et al.
The effect of UV irradiation of methotrexate was investigated by steady state absorption and fluorescence spectroscopy. Major modifications on absorption bands were detected upon irradiation fluence greater than 59J/cm2. In addition the irradiated solutions become strongly fluorescent. The detected changes are not linear with the exposure time suggesting that the photo-induced chemical processes are complex.
Implications of low-power He-Ne laser and monochromatic red light biostimulation in the metabolism of proteins and glucosides
I. Onac, L. Pop, Rodica Ungur, et al.
We checked the changes occurring in the metabolism of proteins (seric cholinesterase, total proteins) and in the metabolism of glycosides (seric glucose) in Cavia cobaia. A simple blind study was carried out and the results were checked on the first, tenth and twentieth days of treatment. The data thus obtained were graphically represented and statistically processed according to the Duncan test. The technique and treatment doses were similar and they were compared with the data obtained from controls and environment controls. In the groups biostimulated with He-Ne laser, seric cholinesterase levels increased proportionally with the dose reaching a peak on day 10, which was not the case with the controls. Monochromatic red light caused a similar but quantitatively lower effect. The same results were obtained in the case of seric proteins as well, however, the effect did not depend on the dose and it was less significant statistically than in the case of seric cholinesterase both in laser treated and in monochromatic red light treated groups.
Experimental aspects concerning the laser action on the living tissue
Tavi Ciuchita, Ciprian Antipa, Constantin S. Stanescu, et al.
The paper presents some experimental methods of the treatment and investigation aspects and results concerning the interaction of the low energy laser (LEL) with living tissue in the treatment of some skin diseases: lichen ruber planus (LP) and infectious finger pulpits (IFP), scalp alopecia (SA) and crural ulcers (CU). We concluded that LEL therapy is a useful complementary method in the treatments of these skin diseases .
Molecular excitations with change of shape
Gabriel Stanescu, Ioana Biloiu
An explanation of the polyatomic molecules shape changing in certain excited states using the group theory is presented. The method of electron configurations, deduced from molecular orbital theory was used. It is possible to see the mechanism that makes a molecule change its shape in some excited states by the correlation between the united atom orbitals, the molecular orbitals and the separated atoms orbitals. The hybridization of the atomic orbitals is favored in some symmetries of the molecule. As a direct result, the changing of the molecule symmetry is given by the filling of these orbitals with electrons.
Optical transmission of fatty acids mixtures
Maria Honciuc, Eugenia G. Carbunescu, Floriana Iova
In this paper we present the visible and infrared transmission of the fatty acids systems: arachidonic, arachidonic - arachidic (2:1) percent in weight and arachidonic - arachidic (1:2) percent in weight. The arachidonic acid prepared in a thin layer of 24 micrometers has a smectic liquid crystal behavior, with fiber texture. The arachidonic and arachidic systems in weight percentage (2:1) and (1:2) present, in a thin layer, the smectic C liquid crystal state. Our studies put in evidence the essential differences between the transmission of these systems in the visible and infrared range. The arachidonic acid presents a high absorption in the range (lambda) is a member of the set (330 divided by 350)nm. Within the range (lambda) is a member of the set (340 divided by 800)nm the absorption has high oscillations with a relatively constant period that can be interpreted based on the modification of the electron positions in the double bounds. All systems present a high absorption in the far infrared region (lambda) is a member of the set (2 divided by 20)micrometers . There are presented the results concerning the behavior of arachidonic acid under an external field, the influence of the monochromatic radiation upon the electric behavior and is emphasized the essential role of the percentage of arachidic acid in the modification of the electric state of the system.
Physicist's simple access to protein structures: the computer program WHAT IF
Brigitte Altenberg-Greulich, Stephan G. Zech, Dietmar Stehlik, et al.
We describe the computer program WHAT IF and its application to two physical examples. For the DNA binding protein, OCT-1 (pou domain) the location of amino acids with a sidechain amino group is shown. Such knowledge is required when staining this molecule with a fluorescence dye, which binds chemically to the amino terminus as well as amino groups in sidechains. The program shows that most sidechain amino groups are protected when DNA is bound to OCT-1, allowing selective staining of the amino terminal NH2 group. A protein stained this way can be used in fluorescence spectroscopic studies on function aspects of OCT-1.
Optoelectronics
icon_mobile_dropdown
Combination of guided wave and free-space micro-optics for a new optical backplane concept
I. Frese, Stefan Kufner, Maria Kufner, et al.
High data rates, immunity against electro-magnetical interference and the ability for low-cost mass production are the basic reasons for the replacement of electrical wire networks by their optical equivalents. The highly integrated micro-optical backplane concepts discussed in this paper are based on a combination of guided wave and free space micro- optical elements and are compatible to multi-fiber MT connectors. The required positioning accuracy of the micro- optical elements is guaranteed by the LIGA technique. Monolithic integration in one substrate allows to reduce the degree of freedom for critical alignment.
Control of photocurrent in semiconductors through femtosecond pulses
Valerica Ninulescu, Paul E. Sterian, Mihaela A. Ghelmez, et al.
Phase-coherent control of photocurrent magnitude and directionality in semiconductors using lineraly chirped pulses is proposed and analysed. Measurable photocurrents can be generated for the pulsewidth shorter than the dephasing time of the excited carriers.
Remote sensing data for urban air quality assessment
The study focuses on the assessment of the potentialities of remote sensing data to study urban micro-climate and air quality. In urban areas, air quality is quite dependent on the air flow drag which is influenced by the aerodynamic roughness parameters of the ground. These parameters are linked to the urban structural features and their topologies. They characterize the evolution of the vertical wind profile with the altitude. Most of all SAR ERS-1 and ERS-2 images with a time variability are very useful for morphological urban structures extraction. To extract structural features spectral signatures of different terrain features are used to separate surface units for eastern part of Bucharest region and to classify them into general categories. Remote sensing data could be used for the mapping of the air quality parameters, the dust particulates concentration and the apparent temperature being highly correlated for Landsat TM6 data (thermal infrared band data). Spatial distribution of the dust particulates can be mapped for Bucharest metropolitan area based on LANDSAT TM and SPOT data.
Characterization of anodic oxide for GaAs-based laser diodes
Rodica V. Ghita, D. Pantelica, F. Negoita, et al.
Anodic film oxide was deposited in a alcohol-glycol-water (AGW) solution on n-GaAs for passivation purpose in stripe technology for laser diodes. The characteristics of anodic oxide were measured by scanning electron microscopy (SEM), Rutherford backscattering (RBS) analysis and elastic recoil detection (ERD) techniques. The result indicates a complex oxide structure in the phase base Ga2O3:As2O3(1:1) joined together with carbon bonds. Due to the presence of carbon in anodic oxide, laser diodes are exposed to rapid degradation during operation.
Optoelectronics silicon on insulator integrated circuits by porous silicon technology
M. Balucani, G. Lamedica, V. Bondarenko, et al.
This work reports on the CMOS-SOI devices based on porous silicon technology (PST) opening the possibility of wafer scale integration realizing on-chip optoelectronic integrated circuits by the PST. Silicon on insulator (SOI) structure based on the preferential anodization of n+ layer within n-/n+/n- were realized. Standard n-type Si (100) have been used as initial substrates. N+ layer have been formed by Sb ion implantation into the front and backside of the substrates followed by annealing. Then an epitaxial layer has been grown on the front of the wafers and projection photolithography using reactive ion etching of both the mask and the epitaxial layer has been used to define three dimensional pattern of islands wherein device components are formed. Characteristics and device layout are presented for partially depleted devices used to build ring oscillator showing that a 1.2 micron resolution in SOI porous silicon technology is comparable with a 0.5 micron CMOS technology.
Influence of a-Si:H buffer layers on the properties of CNx materials
B. Mitu, Gheorghe H. Dinescu, E. Aldea, et al.
On the basis of ab initio calculations, the (alpha) , (beta) - C3N4 crystalline compounds have been proposed as promising materials for optical applications in ultraviolet and visible. However, these crystalline forms of carbon nitride have been hardly obtained, mostly the formation of amorphous material being noticed. Previously, deposition of amorphous carbon nitride from an RF plasma jet operating in nitrogen with graphite electrodes was reported. This work reports on the deposition and characterization of carbon nitride thin films by RF nitrogen plasma beam with graphite electrodes either on glass on crystalline Si or on intermediate a-Si:H buffer layers. The layers properties (composition, crystallinity and absorption in ultraviolet, visible and infrared) have been studied by x-ray photoelectron spectroscopy (XPS), FTIR (Fourier transform infrared spectroscopy) and UV-VIS absorption, energy dispersive x-ray analysis (EDX) and x-ray diffraction (XRD) techniques. It is shown that amorphous carbon nitride materials with variable optical bandgap in the range 1.2-3.5 eV can be obtained. Also, the formation of an intermediate SiCN interlayer and the promotion of crystallinity in CNx films, due to buffer layer presence, is proved.
Characterization of the photostructurable media from carbazol-containing copolymers and thermo-cross-linking media from vynil-containing copolymers
Valeriu V. Bivol, Stephan V. Robu, Andrei M. Andriesh, et al.
Cross-linking and structurable polymer photosensitive materials have been studied for many years and they are widely used for optical recording of information. After the investigation of the photo-chemical and photo-physical processes in various systems, it appears that the chemical structure of the polymer matrix plays an essential role in the process of reaction that takes place upon irradiation by a laser beam. The results of experiments that were conducted to investigate the modification of the absorption with the time of exposure, modification of the degree of photo- structuring with time, the dependence of the photosensitivity of thickness and other characteristics are presented in this paper. Some of the applications of the results concerning the hardening of the cross-linking polymers with the scope to improve the mechanical properties of the surface relief image (hardness, strength, adhesive stability) and the possibilities to make copies by the hot stamping method are also presented.
Objective lens design for image intensifier night vision sight
Marinica Mirzu, Stefan Cantaragiu, Liviu Cosereanu, et al.
The paper presents some considerations about designing optical components in electro-optical image intensifier night vision systems. In such systems very important is the modulation transfer function (MTF) at the interest spatial frequencies (0...50 cy/mm), instead of RMS spot size. The relationship between imposed observation ranges and the MTF of the optical system is through the signal to noise ratio (SNR) of the entire electro-optical system. To illustrate these considerations we present an example of work in the design of the objective lens for an electro-optical image intensifier night vision sight.
LISA: lidar with integrated spectroscopy and anemometry
Numerical models are widely used to study the complex phenomenon of air pollution. Nevertheless, their predictions should be compared with range- and time-resolved measurements. In this paper, we suggest LISA (Lidar with Integrated Spectroscopy and Anemometry), a laser radar able to simultaneously retrieve the profiles of aerosol loads, wind vectors, and trace gases. Six beams are emitted in the atmosphere: two are slanting and four are vertical. The beam propagation at different wavelengths gives information on the aerosol load. The wind vector is reconstructed from its components along the three beam directions. The concentration of a trace gas is obtained by differential absorption.
Optical Sensors and Metrology
icon_mobile_dropdown
Optical recognition of three-dimensional objects with in-plane rotation invariance
In this paper we present a real-time system for three- dimensional (3D) object recognition. It is based on the use of the Fourier transform profilometry technique and a joint transform correlator. The projection of a regular fringe pattern onto the 3D object surface permits us to obtain a distorted grating pattern that carries all the 3D information of the object. The analysis of such patterns is the basis of the method for recognizing 3D objects in real time. Later, by encoding with a fringe pattern a single component of the circular harmonic expansion derived from the object to be detected, a rotation-invariant 3D object recognition is also demonstrated. The whole experimental setup is robust and can be constructed with simple equipment. The experimental results demonstrate the theory and show the utility of the proposed method.
Interferometric detection of photothermal effects in uranyl optical glass
Alexandru M. Preda, Constantin P. Cristescu, Ion M. Popescu, et al.
In this paper we present a sensitive photothermal interferometric detection technique using a Wollaston prism. The interference fringe pattern is formed by overlapping of the ordinary and extraordinary beams with adjustable intensities by a linear polarizer. The interferometric montage is made both for the pump beam (Ar-ion laser) and the probe beam (He-Ne laser). From the analysis of the interference patterns obtained separately for the two beams, we calculate the absolute change of the refractive index in the middle of the heated zone of an uranyl-doped optical glass, as well as the average transverse refractive index gradient induced by the pump laser. The experimental results are interpreted in terms of a Gaussian beam propagating through a weak absorptive medium whose refractive index is thermally modified by the pump beam.
Gaussian to rectangular light beam redistribution using computer-generated phase elements
Dan Cojoc, Luca Businaro, Enzo M. Di Fabrizio, et al.
Some considerations on the design of computer generated phase elements applied to the intensity redistribution of Gaussian light beams are presented in this paper. The computer generated phase elements are designed using an iterative transform algorithm for Fresnel domain. Parameters which influence the performances of these algorithms and the computation time are discussed. Results obtained by computer simulations are presented for three different Gaussian beam shaping (flat-top, 2 shifted gaussians, acronym.)
Three-dimensional infrared laser vision system for road surface features analysis
Liviu Bursanescu, Mihaela Bursanescu, Maher Hamdi, et al.
A mobile (truck-mounted) imaging system uses laser-based technology to obtain accurate quantitative data in real time and at high speeds regarding the conditions of road and highway surfaces. Specifically, the GIE Technologies laser vision system integrates a three-dimensional laser-sensing imaging sensor array to map the cracks, ruts and roughness of road surfaces. The LaserVision System simultaneously records a three-dimensional information along with photometric data using the same set of Biris (bi-iris) sensors. These sensors were developed for this application by engineers at GIE Technologies Inc. under exclusive license from the National Research Council (Ottawa, Canada). They rely on a combination of defocusing and triangulation principles to record 3D information about a test surface. The Biris approach, for a mobile pavement testing system, offers several performance advantages in comparison to other sensing methods. Most important, a Biris sensor uses all- solid-state components with no moving parts. This rugged design is highly resistant to misalignment and performs well in a moving, continuously vibrating vehicle. The photometric (intensity) information provides complementary data where ranging alone proves insufficient, as when detecting pavement markings, sealed road cracks or patches. In addition, the range analysis uses simple trigonometry to obtain real-time performance.
Switched-mode laser power supply
Constantin Blanaru
A switched-mode laser power supply (SMPS) for driving He-Ne lasers is presented. It uses an integrated SMPS control circuit to drive a flyback converter running in discontinuous current mode. The IC controls the SMPS power throughput and regulation by pulse-width modulation (PWM) of a fixed frequency drive signal for a bipolar power switching transistor. PWM control is achieved by varying the duty factor of the SMPS power transistor switching between 17.5% and 40%. The SMPS operates from a main input voltage range of (185-250) Vrms/50 Hz with an efficiency higher than 90%.
Frequency comparison involving the Romanian primary length standard RO.1 within the framework of the EUROMET Project #498
Gheorghe Popescu
An international frequency comparison was carried out at the Bundesamt fuer Eich- und Vermessungswessen (BEV), Vienna, within the framework of the EUROMET Project #498 from August 29 to September 5, 1999. The frequency differences obtained when the RO.1 laser from the National Institute for Laser, Plasma and Radiation Physics (NILPRP), Romania, was compared with five lasers from Austria (BEV1), Czech Republic (PLD1), France (BIPM3), Poland (GUM1) and Hungary (OMH1) are reported. Frequency differences were computed by using the matrix determinations for the group d, e, f, g. Considering the frequency differences measured for a group of three lasers compared to each other, we call the closing frequency the difference between measured and expected frequency difference (resulting from the previous two measurements). For the RO1 laser, when the BIPM3 laser was the reference laser, the closing frequencies range from +8.1 kHz to - 3.8 kHz. The relative Allan standard deviation was used to express the frequency stability and resulted 3.8 parts in 1012 for 100 s sampling time and 14000 s duration of the measurements. The averaged offset frequency relative to the BIPM4 stationary laser was 5.6 kHz and the standard deviation was 9.9 kHz.
Experimental evidence of the phase behavior at the waist of a gaussian laser beam
Adrian Dobroiu, Victor Nascov, Dan Apostol, et al.
The phenomenon of phase retardation in the waist region of a gaussian beam (known as the Guoy effect) is described and demonstrated in the visible wavelength range. Two gaussian beams, originating from the same laser, are made to interfere in a region around the waist of one of them and far from the waist of the other. The relative phase is measured by processing the interference patterns recorded at different locations on the axis. A comparison with the theoretical results is carried out.
Frequency-looked He-Ne laser system: stability measurements
Gheorghe Popescu, Sorin Martoiu
An iodine-stabilized He-Ne laser and a short external-mirror laser operating in single-longitudinal mode were used to form a master-slave laser system at 633-nm wavelength. As compared to the beam from the master laser, the beam of the slave laser is frequency-modulation-free and has a higher power. Also, the slave laser oscillation frequency is offset-locked in iodine-stabilized He-Ne laser by using a fast phase lock loop (PLL) circuit. The fluctuations of the frequency offset between the master and the slave lasers were less than 5 parts in 1013 with a 100 s gate time (the relative standard Allan variance was determined measuring the beat frequency between the master laser and the slave laser for different gate times while the iodine- stabilized laser was locked to different lines from the group d, e, f, g). The system proved a fast response and allows for a frequency offset of up to 300 MHz.
Automatic digital processing of Newton's rings fringe patterns
Victor Nascov, Adrian Dobroiu, Dan Apostol, et al.
A numeric algorithm for processing Newton's rings fringe patterns is presented. The interference images of this type have a characteristic appearance which can be described mathematically by a function depending on a set of parameters. The algorithm consists in finding the parameters of this mathematical expression by means of fitting the pattern using the least squares method, specially implemented with an iterative procedure. Unlike other processing methods which also use statistical calculus, this algorithm efficiently utilizes the whole information contained in the image and ensures the highest degree of accuracy, in given statistical fluctuation conditions affecting the image.
Filtering possibilities based on oscillating systems for optoelectronic signals
Cristian I. Toma
Usually filtering and sampling devices for optoelectronic signals consists of low-pass filters represented by an asymptotically stable system (of first or second order). Many times an integration of the filter output over a certain time interval is added. However, such a structure is very sensitive at the random variations of the integration period. This paper will show that for obtaining a filtering and sampling device less sensitive at these random variables we have to use a filter represented by an oscillating system. Mathematical aspects connected with the number of state-variables are also presented.
Errors investigation in dimensional measurement by laser beam scanning
Constantin Blanaru, Dan Apostol, Victor S. Damian, et al.
When dimensional measurement of a body are performed by laser beam scanning, some sources of errors must be taken into account and evaluated. They relate to: laser noise, non-linearity and reproducibility of the scanner movement, optics aberrations, body edge detection, data processing. The paper presents the results of error investigation in contact-less dimensional measurement by laser beam scanning.
Laser beam characterization under PC control
Dan G. Sporea, Alexandru Ivan, Tiberiu Visan, et al.
Laser products for medical or industrial use have to be evaluated both for their performances (output power/energy power/energy density, bean characteristics, etc.,) and from laser safety point of view. This paper presents an integrated setup for characterization of the laser systems, by connecting, through a dedicated software, stand alone measurement devices. In our set-up two Spiricon laser beam analyzers: LBA 100 and LBA 300-PC as well as an Orphir LaserStar power/energy meter work under a PC control. Some of the software involved was developed by using the LabVIEW 5.0 graphically programming environment, and allows the user to remotely control the measurement process by virtual instruments.
Ultraviolet radiation sensors on the basis of semiconductors
Valerian Dorogan, Tatiana Vieru, Mihail Manole, et al.
This paper deals with elaborating and manufacturing of new structure of UV radiation sensors on the basis of single- crystal Si. The structure consists of two photoactive cells, differentially connected to loading resistor. One cell is covered with a layer, transparent for visible and IR radiation and non-transparent for UV radiation. Differential connection excludes the common for both cells components. Thus, the photocurrent of differential sensor is proportional only to UV radiation intensity.
A/D acquisition system for an iodine-stabilized He-Ne laser
Gheorghe Popescu, Victor Andrei
An A / D acquisition system was developed for an iodine- stabilized He-Ne laser for better characterization of the operating parameters and an automatic frequency locking on the iodine feature was the aim of our experimental work. A dedicated software was developed to enable the automatic acquisition circuitry to locate and lock onto the chosen iodine-peak from the groups d, e, f, g, or h, i, j, by making use of second and third harmonic components of the detected signal. More, a warning signal is sent by the PC AT compatible computer to the electronic controller to acknowledge the lock condition.
Optical Components
icon_mobile_dropdown
Laser damage resistance of thin films for ultraviolet optical components
The laser induced damage in optical coatings plays a limiting role in the laser reliability. Either the laser cavity mirrors and the optical components employed outside the cavity are often damaged by the laser radiation, delivered by high power lasers. Their resistance becomes more critical at shorter wavelengths, therefore the research is focused on the ultraviolet region where excimer lasers are finding many applications. Laser damage studies were performed at 248 nm (KrF laser) and 308 nm (XeCl laser) on MgF2, HfO2 and SiO2 films and multilayer coatings. Results about the dependence of the damage threshold on both the deposition technique and standing-wave electric field profile inside the coating, are reported.
Optical homogeneity and growth defects in sapphire crystals grown by different methods
C. Logofatu, I. Licea, N. Mincu, et al.
To investigate the optical homogeneity of crystals some methods based on the analysis of the laser beams interacting with a sample have been recently proposed. The emergent beam is acquired by a data acquisition/image processing system which offers the possibility for both local and global analysis of the sample. Combined with microscopy techniques these methods enable the study of submicron defects such as scattering centers, clusters of punctual defects, microcracks. A map of the absorption coefficient (alpha) equals(alpha) (x,y) can be obtained by recording the transmitted light when scanning the sample with the laser beam. This result is particularly useful for determining some growth parameters because spatial variation of the absorption coefficient is a consequence of thermal oscillations in the crystallization system. Our paper is a short study on the optical homogeneity of sapphire crystals grown by different techniques as related to the particular defects induced by the growth process. Laser beam analysis has been mainly employed to characterize the samples. The results provide important information on the dynamics of the crystallization interface during the growth processes, on the number and types of growth defects, foreign phase precipitations, inclusions, thermal stress, etc., which may help with optimization of the growth parameters.
Efficiency analysis of periodic diffractive optical elements: suitability of various approaches
Uriel Levy, Emanuel Marom, David Mendlovic
Improved manufacturing techniques make diffractive optics a very common element in modern optical systems. Exact estimates of their operating efficiency is of utmost importance. Thus the diffraction efficiency of a multi-level blazed grating is evaluated two ways: analytic computation using the rigorous coupled wave analysis and approximation based on the thin element model. According to the obtained results, the computational error for a periodic diffractive optic element is calculated as a function of the period- length to wavelength ratio as well as the dependence on the phase modulation depth, and an error map is developed. An approximated model based on the thin element model, in conjunction with shadow blocking, whereby some of the rays are blocked by the surface corrugation, is suggested. Using the above approach, an expression for the diffraction efficiency is derived, yielding very good results for moderate period-length to wavelength ratios with minimal computational complexity. The suggested approach is thus advantageous in such regimes, whereas the exact rigorous calculations requires massive computation effort and the classical thin element approximation is not accurate enough.
Heat transfer in IR optical components during CO2 laser irradiation
It is of great importance from the experimental point of view, to understand the thermal behavior of the optical components during how power/energy laser irradiation. The study of the heat transfer in the sample volume is necessary in designing and manufacturing high quality optical components. In this context, we discuss the surface heat transfer coefficients influence on the temperature profile, during CO2 laser irradiation of homogeneous optical components. The assumption of zero heat transfer across the sample radial longitudinal sections is also analyzed. Thermal profiles deduced from the heat diffusion equation are plotted for different heat transfer values.
Optimization of optical coatings in optical systems
Gheorghe Honciuc, Danut Ursu, Gh. Singurel
The spectral response of a non-uniform optical coating in a particular optical system is analyzed. The optical coating in the optical system is optimized having as targets the spectral responses (integral reflection factors) of the coating deposited on a diopter in a particular optical system. A conversation is established between the designing program for optical coatings and the designing program for optical systems. The designing program for optical coatings communicates to the designing program for optical systems the coating and the targets to be optimized. The designing program for optical systems evaluates the merit function and communicates it to the designing program for optical coatings, which accordingly modifies the optical coating parameters to attain an optimum, depending on the merit function evolution. The process is repeated until the merit function reaches an extreme.