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Proceedings Paper

TGA/FTIR and DSC/FTIR: combined approaches to solving problems
Author(s): David A. C. Compton; Jay R. Powell; Richard A. Crocombe
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Paper Abstract

Thermal analysis of complex samples has been greatly assisted by the coupling of FT-IR analysis to the TA experiment, and evolved gas analysis by infrared spectroscopy has been very successful in combined TGA/FT-IR experiments. During a combined DSC/FT-IR experiment the FT-IR analysis is performed on the sample itself, by using an infrared transmitting microscope. A curing reaction and thermal changes in a polymer are used to demonstrate the use of a combined DSC/FT-IR system. By combining a simultaneous TGA/DSC instrument with FT-IR evolved gas analysis, we are now able to obtain three sets of complementary information, on the same sample, in one experiment. A study of the thermal behavior of zinc stearate is reported by using TGA/DSC/FT-IR.

Paper Details

Date Published: 1 March 1992
PDF: 2 pages
Proc. SPIE 1575, 8th Intl Conf on Fourier Transform Spectroscopy, (1 March 1992); doi: 10.1117/12.56310
Show Author Affiliations
David A. C. Compton, Bio-Rad Labs., Inc. (United States)
Jay R. Powell, Bio-Rad Labs., Inc. (United States)
Richard A. Crocombe, Bio-Rad Labs., Inc. (United States)

Published in SPIE Proceedings Vol. 1575:
8th Intl Conf on Fourier Transform Spectroscopy
Herbert Michael Heise; Ernst Heiner Korte; Heinz W. Siesler, Editor(s)

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